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By C.E.R. Jones (Eds.)
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Extra resources for Analytical Pyrolysis
The availability of precursor ions of unique elemental and isotopic compositions will remove a serious source of ambiguity for many s t u d i e s . Note that the precursor ions can a l s o be limited to a very narrow range of kinetic energies through narrowing of the b e t a - s l i t of MS-I. The range of precursor ion kinetic energies has been the source of ambiguity, especially in previous MI s t u d i e s , and methods to correct for the energy spread had been proposed [28, 2 9 ] . With the narrow b e t a - and e x i t - s l i t MS-I, a metastable decomposition involving a unique energy r e l e a s e should give a pair of relatively narrow peaks centered around the calculated mass p o s i t i o n .
M . R. Lester, 11 Metastable I o n s " , Elsevier, Amsterdam, 1973. 10 F . W . McLafferty, P . F . Bente, III, R. Kornfeld, S . - C . T s a i , and I . Howe, J. Am. Chem. S o c , 95(1973)2120. 11 F . W . McLafferty, R. Kornfeld, W . F . Haddon, K. Levsen, I . Sakai, P . F . Bente, III, S . - C . Tsai, and H . D . R . Schuddemage, J. Am. Chem. S o c , 95(1973)3886. 48 12 K. Levsen and H . D . Beckey, Org. , 9(1974)570. 13 H . L . C . Meuzelaar, N . M . M . Nibbering, and H . H . Tuithof, September 1975, private communication.
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Analytical Pyrolysis by C.E.R. Jones (Eds.)